Measuring Couplings in Crowded NMR Spectra: Pure Shift NMR with Multiplet Analysis

Research output: Contribution to journalArticle

Abstract

The PSYCHE method for pure shift NMR is exploited to generate 2D J spectra with full decoupling in one dimension and multiplet structure in the other, allowing spin–spin coupling constants to be measured even in very crowded spectra. Significant improvements over existing techniques are demonstrated for the hormones estradiol and androstenedione.

Bibliographical metadata

Original languageEnglish
Pages (from-to)15410-15413
Number of pages4
JournalChemical Communications
Volume51
Issue number84
DOIs
StatePublished - 27 Aug 2015