A new pulse sequence, CHORUS Oneshot, allows measurement of diffusion-ordered spectroscopy (DOSY) spectra over the full chemical shift range of 19F for the first time. Frequency-swept pulses are used to give very broadband excitation and refocusing; the sequence is a prototype for a large family of very broadband liquid state NMR methods. Full experimental data, pulse sequences, pulse shapes are given in Bruker TopSpin format.
|Date made available||15 Feb 2016|
|Publisher||University of Manchester|
|Date of data production||31 Jan 2016|